Perform first real-world synthesis experiment

[jmeyer1980]

Description

Execute the first real alloy synthesis based on model recommendations to close the loop and validate the entire system.

Tasks

• Run model to generate top 10 candidate alloys
• Select highest-confidence, highest-priority candidate
• Review with metallurgist: does this make sense?
• Obtain materials (check availability and cost)
• Follow synthesis procedure from CSV export:
  • Weigh out feedstock masses exactly as specified
  • Use recommended method (arc melting, furnace, etc.)
  • Follow temperature and atmosphere specifications
  • Document time and actual cost
• Characterize result (XRD, SEM, hardness test, etc.)
• Log outcome in system:
  • Success/Partial/Failed
  • Notes on what happened
  • Deviations from plan
• Compare predicted vs actual outcome
• Document lessons learned

Acceptance Criteria

• At least one alloy is physically synthesized
• Outcome (success or failure) is logged
• Experience informs model improvements
• Documentation captures the full experiment
• Team has confidence in using system for future experiments

Estimate: 4-8 hours (actual lab work)